Analysis of Dimer Impurity in Polyamidoamine Dendrimer Solutions by Small-angle Neutron Scattering

Small angle neutron scattering

Small Angle Neutron Scattering (SANS) is a technique that enables to probe the 3-D structure of materials on a typical size range lying from ∼ 1 nm up to ∼ a few 100 nm, the obtained information being statistically averaged on a sample whose volume is ∼ 1 cm3. This very rich technique enables to make a full structural characterization of a given object of nanometric dimensions (radius of gyrati...

Assess the Intramolecular Cavity of a PAMAM Dendrimer in Aqueous Solution by Small-Angle Neutron Scattering

We present a contrast variation small-angle neutron scattering (SANS) study of a series of neutral PAMAM dendrimers in aqueous solutions using three different generations (G4-6) at a concentration of about 10 mg/mL. Varying the solvent hydrogen-deuterium ratio, the scattering contributions from the water molecules and the constituent components of PAMAM dendrimer can be determined. Using an ana...

MnO 3 by small angle neutron scattering

Longitudinal polarization analysis in small-angle neutron scattering

Due to recent progress in the development of He spin filters, it has only now become possible to perform routinely longitudinal (one-dimensional) neutron-spin analysis (POLARIS) in small-angle neutron scattering (SANS) experiments. It is the purpose of this article to provide a brief introduction into the technique and to discuss first experimental data. In particular, for the most common scatt...

Neutron small angle scattering of hemoglobin.

Neutron small angle scattering experiments were performed on human hemoglobin in various mixtures of Hz0 and DzO. It was possible to observe the inter-particle effect without corrections for resolution and to verify the first minimum and the secondary maximum in accordance with the theoretical scattering curve. The accuracy in determining the radius of gyration has been improved over that deter...